Analysis of Acrylamide by GC-MS

Authors

  • R. Papoušek Regional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacký University, Olomouc
  • P. Nováková Regional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacký University, Olomouc
  • E. Marková Regional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacký University, Olomouc
  • P. Barták Regional Centre of Advanced Technologies and Materials, Department of Analytical Chemistry, Faculty of Science, Palacký University, Olomouc

Keywords:

acrylamide, derivatization, bromination, 2-bromopropenamide, gas chromatography, mass spectrometry, GC-MS

Abstract

The study deals with the GC-MS determination of acrylamide in various matrices. The proposed method involves bromination of acrylamide to 2,3-dibromo­propanamide, its conversion to 2-bromopropenamide and the GC-MS determination. The method was used for the determination of acrylamide in water, gaseous products of combustion and in food such as potato chips and cookies. The measured concentrations of acrylamide ranged from 46 to 1980 µg kg–1 the highest levels being found in ground coffee and tobacco smoke.

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Published

2013-03-15

How to Cite

Papoušek, R., Nováková, P., Marková, E., & Barták, P. (2013). Analysis of Acrylamide by GC-MS. Chemické Listy, 107(3), 255–260. Retrieved from http://w.chemicke-listy.cz/ojs3/index.php/chemicke-listy/article/view/752

Issue

Vol. 107 No. 3 (2013)

Section

Articles